How to isolate the resin and Boswellic acids from select Frankincense oleoresins with water
Boswellia Papyrifera-Isolated Resin-Boswellic acids-
Lately, we have been hearing a lot about the anti-inflammatory and anti-cancer compounds found in the frankincense family. The most publicized recently are the Boswellic acids and AKBA, or acetyl-keto-beta-boswellic acid, pentacyclic triterpenes found in some species of Frankincense which make up a significant part of the resin in these oleo-gum-resins. The motivation for the increase in research, and much of the funding, from what I can see, is largely due the projected profit perceived by pharmaceutical companies. This isn’t necessarily a bad thing, since it provides the impetus for discovery, progress and knowledge, but good to keep in mind nonetheless.
With a rapidly growing aging population in the west, an increase in chronic inflammatory diseases such as arthritis, rheumatism, inflammatory bowel disease, and various cancers, the market is receptive. There are theories that most if not all age-related degenerative conditions are directly associated with inflammation. Frankincense’s history of use in traditional eastern medical systems as an anti-inflammatory makes it an excellent candidate for modern applications..
Frankincense Sacra/Carterii tree in the wild
Besides hearing about Boswellic acids in groundbreaking studies, some essential oil companies advertise that their distilled essential oils of Frankincense contain a high percent of Boswellic acids. This is misleading. Some essential oils of Frankincense may have a higher percent of Boswellic acids than other essential oils of Frankincense, but the Boswellic acids are not found in the essential oils except in trace amounts. They are found in the heavy resin portion and cannot be distilled into the essential oils except in minute quantities. Like politics, statistics in advertising can be misleading.
The Boswellic acids are heavy molecules called triterpenes, and while many beneficial compounds are light enough to separate themselves from the frankincense oleo-gum-resin when heated during the distillation process, the Boswellic acids are not. They make up the heavier resin portion. This is not to say that the essential oil of Frankincense is not a wonderful therapeutic oil with many valuable compounds and health benefits, but that when it comes to Boswellic acid content, it can only have trace amounts unless Boswellic acids were added to it manually and then it would no longer be an essential oil, but an oleoresin..
Made up mainly of Boswellic acids, and solid at room temperature, the pure resins of Boswellia Sacra/Carterii beneath B. Papyrifera do not distill over with the essential oils.
The only products that can claim with verity to contain significant amounts of Boswellic acids are either the whole raw oleo-gum-resin of certain Frankincense types, or extracts that have been processed with solvents to isolate the resins that contain the Boswellic acids. Boswellic acids are not found in the water-soluble gum portion of Frankincense or the distilled essential oils except as mentioned, in trace amounts.
Claims that the essential oil of Frankincense from any company, contains a high percent of Boswellic acids, that you should ingest their essential oils, or that their oils are “Therapeutic quality”, were developed to market their products and are not put forth in the interest of your edification or wellbeing.
- There is no significant amount of Boswellic acids in any Frankincense essential oil when compared to the quantities naturally present in the unprocessed oleo-gum-resin, the pure resin or the extract.
- You should never ingest essential oils without consulting with a qualified healthcare professional.
We have come to associate the essential oil of any given plant as the quintessence of its healing properties. While this may be true for some plants, it is far from the truth for oleoresins which hold many healing compounds in their undistillable resin portion.
If you would like to extract or isolate the Boswellic acids and the resin portion of Frankincense yourself, there is a simple way you can do this with the right type of Frankincense. Once you have the pure resin it is relatively easy to make a variety of products that utilize and deliver the Boswellic acids. The whole oleo gum resin of Frankincense will not dissolve easily in oil based products due to its water soluble gum content. It will also not dissolve well in water based products due to its oleo and resin components. The solution is to separate the water soluble part from the oil soluble part which is the point of this post and the following method.
Frankincense Papyrifera gum dissolved in water on the right, resin in alcohol on the left ,and distilled essential oils center. Not in their naturally occurring proportions
Recent research has identified Boswellic acids in the resin of 3 types of Frankincense. The number may increase as more research is done on other species. ( See pages 125-127) http://scidok.sulb.uni-saarland.de/volltexte/2012/4999/pdf/Dissertation_Fertig_211112.pdf
- Boswellia Papyrifera from Ethiopia, Eritrea, Kenya and Sudan.
- Boswellia Seratta from India.
- Boswellia Sacra/Carterii, (one and the same tree), from Somalia, Kenya, Oman and Yemen.
A visual comparison of 5 types of Frankincense-Boswellia
A simple and safe method to isolate the resin and Boswellic acids in Frankincense
While different solvents can be used to isolate the resin and Boswellic acid portion of Frankincense, The simplest and safest method is to do so is with water.
30/November/2015-Since writing this post, I have developed an easier/better method for separating the resin portion and the Boswellic acids from the whole oleo gum resin. If you are revisiting this page, I hope you find the following process simpler and more satisfying.
- Take 100-500 grams of fresh Frankincense.
- In a stainless steel, Teflon coated or glass pot, bring at least 10 liters of water to a boil. More than this is just fine.
- Place a stainless steel sieve or colander with a fine mesh about 1/2 submerged in the water. Ideally, use a sieve that will rest on the edge of the pot securely, otherwise you will have to hold it at the right height through the process and you will need an extra hand.
- When it is at a full boil, gently add 100 to 500 grams of one of the 3 aforementioned types of Frankincense into the suspended sieve, careful to not splash boiling water on yourself. It is fine if the resin sits partially above the water, it will soon settle.
- With a wooden spoon or some other utensil, gently run the submerged resin granules back and forth through the boiling water allowing the water to wash over them all and dissolve them.
- The water soluble gum will dissolve and disperse in the water while the pure oleoresin, the resin with the essential oils, will exit and float around the outside of the sieve. The bark and other foreign matter will collect in the sieve and not pass to the water.
- Once most of the resin is floating on the surface of the water, it will also push its way back into the sieve. To address this, lift the sieve higher and allow the rest of the resin to exit the sieve. At this point you may need help running the utensil back and forth gently forcing the resin through into the water.
- When the sieve is empty of gum and water, set it aside.
- Skim/scoop out all the resin that is floating in the pot into a separate preferably stainless steel bowl. I use a small colander/sieve that captures more resin than water for this purpose. It’s ok if you transfer water into the bowl with the resin since you can easily pour it off after the resin sets.
- Set the pot of hot water aside to cool. As most of these oleoresins do, they will mostly settle to the bottom of the pot as the temperature drops.
- When the pot has cooled, pour the contents through yet another fine mesh sieve and add the bits of resin you collect in the sieve to your main bowl of collected resin. Pry off as much of the hard resin droplets from your pot.
- Your resin extract still needs to go through the bath once more to remove traces of water soluble gum. When present, they will interfere with the process of making oil based products such as cremes and salves.
- So, repeat the above process of boiling your resin with fresh clean water in the pot.
- Break up the resin into smaller pieces that will melt evenly, and add it to the boiling water.
- Stir it around and you will likely see the water getting a bit cloudy. This is the residual water-soluble gum we want to get rid of.
- It should only take a few minutes of gentle stirring to wash the rest of the gum out of the resin, so after 3-5 minutes of your completely melted resin floating around, you can skim it off as above, and place it in a clean bowl to cool and set.
- Again, let the pot cool and collect any resin you missed.
- Though you could use the resin extract as it is, I put it through one final process to dry it of any residual trapped water. It usually collects water in little pockets and bubbles as it floats around the boiling water.
- To do this, I crush the resin coarsely, exposing as much of it to the air as I can. I stop when the largest chunks are about the size of a pea.
- Place it on a clean Teflon or silicone cookie sheet.
- Preheat the oven to about 120 degrees Centigrade and place the pan in the oven.
- The resin will melt and flow releasing all the water in the form of vapour to the air. I tilt it this way and that to expose any pockets of water while it is hot and mobile.
- It only takes about 2-5 minutes of the resin uniformly melted to dry it and it can be removed from the oven and left to cool.
- When solid and cool, lift from the cookie sheet, break it in pieces if you like and store in ziplock bags or a glass jar. Keep it cool or it may flow a bit and adhere to a glass container.
- I have also used a heat gun, the kind used for stripping paint to melt the resin and remove any trapped water from it. This is an option if you feel like experimenting. If it sizzles a bit it is OK.
You now have a product with a substantial, therapeutically active proportion of Boswellic acids in a concentration much, much higher than you could ever get from a comparable quantity or weight of essential oil without the risk that concentrated essential oils can represent. At the same time you likely have a healthy percent of Frankincense essential oils in their naturally occurring concentration and matrix.
It is a substance that dissolves readily in warm vegetable oils, waxes and alcohol, and lends itself with ease to cremes, oils, salves and more. You know exactly what went into your product from start to finish. You know it wasn’t adulterated along the way, that no solvents, desiccants or fillers were added, and you know you have a 100% natural product.
Though I state it is an easy process, it is rather messy. Here is a visual walkthrough of the above process including some tips on cleanup. – https://apothecarysgarden.com/2016/11/20/extracting-the-resin-and-boswellic-acids-from-frankincense-a-visual-walkthrough/
And remember, always take clear notes. Your future self will thank you.